GLYCINE-1-OCTYL ESTER HYDROCHLORIDE

GLYCINE-1-OCTYL ESTER HYDROCHLORIDE - Names and Identifiers

Name	GLYCINE N-OCTYL ESTER HYDROCHLORIDE
Synonyms	GLYCINE OCTYL ESTER GlycineoctylesterHCl Glycinen-octylesterHCl Octyl 2-aMinoacetate hydrochloride GLYCINE N-OCTYL ESTER HYDROCHLORIDE GLYCINE-1-OCTYL ESTER HYDROCHLORIDE 2-aminoacetic acid octyl ester hydrochloride
CAS	39540-30-2
EINECS	629-934-2

GLYCINE-1-OCTYL ESTER HYDROCHLORIDE - Physico-chemical Properties

Molecular Formula	C10H22ClNO2
Molar Mass	223.74
Melting Point	66-72°C
BRN	3696405
Storage Condition	under inert gas (nitrogen or Argon) at 2-8°C

GLYCINE-1-OCTYL ESTER HYDROCHLORIDE - Risk and Safety

Risk Codes	36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.

GLYCINE-1-OCTYL ESTER HYDROCHLORIDE - Reference Information

application

n-octyl aminoacetate hydrochloride can be used as a pharmaceutical intermediate and can be used in laboratory research and development process and chemical medicine synthesis process.

preparation

100g of industrial aminoacetic acid, 400ml of n-octanol and 11g of catalyst p-toluenesulfonic acid are added to a three-mouth flask, connected to a water separator, condenser tube and stirrer, heated and heated in gradient, and gallic acid is completely dissolved at a certain temperature, the reaction is carried out at a temperature of 105 ℃ until the end of the reaction is reached when no water is generated (the reaction time is 4 hours). Then the reactants are neutralized, washed, crystallized at low temperature, and vacuum filtered to obtain a white needle-like crystalline crude n-octyl aminoacetate; the crude n-octyl aminoacetate is refined, recrystallized, and vacuum After drying, 81.2g of n-octyl aminoacetate is obtained with a content of 99.3%, and then n-octyl aminoacetate hydrochloride is obtained by adding hydrochloric acid.

Last Update：2024-04-10 22:29:15